| Table of Contents | ||
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Process | Time (min) | Comments |
|---|---|---|
1. Obtain a whole-round core section from the core rack | 0.3 | See Preparing Sections & Samples |
2. Locate the appropriate probe for the sample type | 0.5 | |
3. Verify sample identification in software | 0.5 | See Set Measurement Parameters |
4. Configure measurement program | 0.3 | |
5. Perform drift control | 5 | See Making a Measurement |
6. Heat and measure sample | 2 | |
7. 10 minute pause between measurements | 10 | |
8. Repeat steps 5-7 for 2 additional measurements (3 total) | 34 | |
9. Upload results to LIMS | 0.2 | See Uploading Data to LIMS |
10. Check results in LIMS | 1 | |
11. Remove the section and deliver to splitting room | 0.2 | |
Total Time per sample: | 54 (max) |
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- Load ThermCon software in offline mode. Ensure that the Text_ID field is blank.
- Scan the core label using a scanner, then click Verify Sample.
- If login is requested, enter UserName and Password and then click OK.
- The folder path is shown on the screen. Do not close this window during measurement.
- Run TK04 program and choose Measuring > Configuration.
- Set configuration parameters as follows (see figure below):
- Probe Number: serial number of probe to be used in the measurement (Note: results may be wrong by several percent if the wrong serial number is entered or by a factor of ~2 if the wrong type of probe is entered),
- Root Name: six characters or less; suggest Core-Type-Section (no special characters in the root name).
- Serial Number: number of repeat measurements at each measurement point (1–99 single measurements).
- Folder: path for saving data results.
- Heating Power: for the VLQ (needle probe), set to twice the estimated thermal conductivity value of measured sediment. For example, 2–3 is good for sediment. (See the Appendix: TK04 Recommended Heating Power for power guidance.)
- Measuring Time: set to at least 80 s, or for mini HLQ 60 s.
- Click Expert Options to configure Drift Control and Pause in Minutes (see Step 7).
- Enter comments.
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| ANALYSIS | TABLE | NAME (expanded report) | NAME (standard report) | ABOUT TEXT |
| TCON | SAMPLE | Exp | Exp | Exp: expedition number |
| TCON | SAMPLE | Site | Site | Site: site number |
| TCON | SAMPLE | Hole | Hole | Hole: hole number |
| TCON | SAMPLE | Core | Core | Core: core number |
| TCON | SAMPLE | Type | Type | Type: type indicates the coring tool used to recover the core (typical types are F, H, R, X). |
| TCON | SAMPLE | Sect | Sect | Sect: section number |
| TCON | SAMPLE | A/W | A/W | A/W: archive (A) or working (W) section half. |
| TCON | SAMPLE | text_id | Text ID | Text_ID: automatically generated database identifier for a sample, also carried on the printed labels. This identifier is guaranteed to be unique across all samples. |
| TCON | SAMPLE | sample_number | Sample Number: automatically generated database identifier for a sample. This is the primary key of the SAMPLE table. | |
| TCON | SAMPLE | label_id | Label identifier: automatically generated, human readable name for a sample that is printed on labels. This name is not guaranteed unique across all samples. | |
| TCON | SAMPLE | sample_name | Sample name: short name that may be specified for a sample. You can use an advanced filter to narrow your search by this parameter. | |
| TCON | SAMPLE | x_sample_state | Sample state: Single-character identifier always set to "W" for samples; standards can vary. | |
| TCON | SAMPLE | x_project | Project: similar in scope to the expedition number, the difference being that the project is the current cruise, whereas expedition could refer to material/results obtained on previous cruises | |
| TCON | SAMPLE | x_capt_loc | Captured location: "captured location," this field is usually null and is unnecessary because any sample captured on the JR has a sample_number ending in 1, and GCR ending in 2 | |
| TCON | SAMPLE | location | Location: location that sample was taken; this field is usually null and is unnecessary because any sample captured on the JR has a sample_number ending in 1, and GCR ending in 2 | |
| TCON | SAMPLE | x_sampling_tool | Sampling tool: sampling tool used to take the sample (e.g., syringe, spatula) | |
| TCON | SAMPLE | changed_by | Changed by: username of account used to make a change to a sample record | |
| TCON | SAMPLE | changed_on | Changed on: date/time stamp for change made to a sample record | |
| TCON | SAMPLE | sample_type | Sample type: type of sample from a predefined list (e.g., HOLE, CORE, LIQ) | |
| TCON | SAMPLE | x_offset | Offset (m): top offset of sample from top of parent sample, expressed in meters. | |
| TCON | SAMPLE | x_offset_cm | Offset (cm): top offset of sample from top of parent sample, expressed in centimeters. This is a calculated field (offset, converted to cm) | |
| TCON | SAMPLE | x_bottom_offset_cm | Bottom offset (cm): bottom offset of sample from top of parent sample, expressed in centimeters. This is a calculated field (offset + length, converted to cm) | |
| TCON | SAMPLE | x_diameter | Diameter (cm): diameter of sample, usually applied only to CORE, SECT, SHLF, and WRND samples; however this field is null on both Exp. 390 and 393, so it is no longer populated by Sample Master | |
| TCON | SAMPLE | x_orig_len | Original length (m): field for the original length of a sample; not always (or reliably) populated | |
| TCON | SAMPLE | x_length | Length (m): field for the length of a sample [as entered upon creation] | |
| TCON | SAMPLE | x_length_cm | Length (cm): field for the length of a sample. This is a calculated field (length, converted to cm). | |
| TCON | SAMPLE | status | Status: single-character code for the current status of a sample (e.g., active, canceled) | |
| TCON | SAMPLE | old_status | Old status: single-character code for the previous status of a sample; used by the LIME program to restore a canceled sample | |
| TCON | SAMPLE | original_sample | Original sample: field tying a sample below the CORE level to its parent HOLE sample | |
| TCON | SAMPLE | parent_sample | Parent sample: the sample from which this sample was taken (e.g., for PWDR samples, this might be a SHLF or possibly another PWDR) | |
| TCON | SAMPLE | standard | Standard: T/F field to differentiate between samples (standard=F) and QAQC standards (standard=T) | |
| TCON | SAMPLE | login_by | Login by: username of account used to create the sample (can be the LIMS itself [e.g., SHLFs created when a SECT is created]) | |
| TCON | SAMPLE | login_date | Login date: creation date of the sample | |
| TCON | SAMPLE | legacy | Legacy flag: T/F indicator for when a sample is from a previous expedition and is locked/uneditable on this expedition | |
| TCON | TEST | test changed_on | TEST changed on: date/time stamp for a change to a test record. | |
| TCON | TEST | test status | TEST status: single-character code for the current status of a test (e.g., active, in process, canceled) | |
| TCON | TEST | test old_status | TEST old status: single-character code for the previous status of a test; used by the LIME program to restore a canceled test | |
| TCON | TEST | test test_number | Test No. | TEST test number: automatically generated database identifier for a test record. This is the primary key of the TEST table. |
| TCON | TEST | test observation_time | Timestamp (UTC) | Timestamp (UTC): point in time at which the observation was made THIS SHOULD BE A NEW COLUMN ADDED TO THE EXPANDED REPORT. CURRENTLY ONLY REPORTED IN STANDARD REPORT |
| TCON | TEST | test date_received | TEST date received: date/time stamp for the creation of the test record. | |
| TCON | TEST | test instrument | TEST instrument [instrument group]: field that describes the instrument group (most often this applies to loggers with multiple sensors); often obscure (e.g., user_input) | |
| TCON | TEST | test analysis | TEST analysis: analysis code associated with this test (foreign key to the ANALYSIS table) | |
| TCON | TEST | test x_project | TEST project: similar in scope to the expedition number, the difference being that the project is the current cruise, whereas expedition could refer to material/results obtained on previous cruises | |
| TCON | TEST | test sample_number | TEST sample number: the sample_number of the sample to which this test record is attached; a foreign key to the SAMPLE table | |
| TCON | CALCULATED | Depth CSF-A (m) | Depth CSF-A (m) | Depth CSF-A (m): position of observation expressed relative to the top of the hole. |
| TCON | CALCULATED | Depth CSF-B (m) | Depth CSF-B (m) | Depth [other] (m): position of observation expressed relative to the top of the hole. The location is presented in a scale selected by the science party or the report user. |
| TCON | RESULT | contact_value | RESULT contact value (unitless): unitless measure of contact quality between probe and sample | |
| TCON | RESULT | dat_asman_id | RESULT DAT file ASMAN_ID: serial number of the ASMAN link for the .DAT file | |
| TCON | RESULT | dat_filename | RESULT DAT filename: file name of the .DAT file | |
| TCON | RESULT | dwl_asman_id | RESULT DWL file ASMAN_ID: serial number of the ASMAN link for the .DWL file | |
| TCON | RESULT | dwl_filename | RESULT DWL filename: file name of the .DWL file | |
| TCON | RESULT | end_time (s) | RESULT end time (s): the ending time of the experiment in seconds from initialization | |
| TCON | RESULT | erg_asman_id | RESULT ERG file ASMAN_ID: serial number of the ASMAN link for the .ERG file | |
| TCON | RESULT | erg_filename | RESULT ERG filename: file name of the .ERG file | |
| TCON | RESULT | heating_power (W/m) | RESULT heating power (W/m): heating power applied to the sample (it can be useful to reduce this if it is challenging to get a good result) | |
| TCON | RESULT | length_of_time (s) | RESULT length of time (s): duration of the linear portion of the heating experiment, determined by subtracting start time from end time | |
| TCON | RESULT | mdb_asman_id | RESULT MDB file ASMAN_ID: serial number of the ASMAN link for the .MDB file | |
| TCON | RESULT | mdb_filename | RESULT MDB filename: file name of the .MDB file | |
| TCON | RESULT | method | RESULT method: indicates whether the TeKa Berlin SAM method or the linear-calculation TCON method was used | |
| TCON | RESULT | instrument | Instrument | RESULT instrument: name of the instrument used |
| TCON | RESULT | needle_name | Needle name | RESULT needle name: serial number of the needle used (H#### for half-space; V#### for full-space) |
| TCON | RESULT | number_of_solutions | RESULT number of solutions: number of independent valid solutions the SAM method found; the higher this number, the better (and <100 should be carefully checked) | |
| TCON | RESULT | offset (cm) | Offset (cm) | RESULT offset (cm): position of the measurement relative to the top of a sample (generally a section) |
| TCON | RESULT | ssup_asman_id | RESULT spreadsheet uploader ASMAN_ID: serial number of the ASMAN link for the spreadsheet uploader file | |
| TCON | RESULT | ssup_filename | RESULT spreadsheet uploader filename: file name of the spreadsheet uploader file | |
| TCON | RESULT | start_time (s) | RESULT start time (s): the starting time of the experiment in seconds from initialization | |
| TCON | RESULT | therm_con_average (W/(m*K)) | Thermal conductivity mean (W/(m*K)) | RESULT average thermal conductivity (W/(m*K), SAM): mean result of successive thermal conductivity observations using the SAM method |
| TCON | RESULT | therm_con_number | Measurements (no) | RESULT number of measurements (SAM): the number of measurements performed to produce the mean result for the SAM method |
| TCON | RESULT | therm_con_result (W/(m*K)) | Thermal conductivity observations (W/(m*K)) | RESULT individual thermal conductivity (W/(m*K), SAM): individual thermal conductivity measurement using the SAM method |
| TCON | RESULT | therm_con_stdev (W/(m*K)) | Conductivity std. dev (W/(m*K)) | RESULT standard deviation (W/(m*K), SAM): standard deviation of the averaged results from the SAM method |
| TCON | RESULT | therm_con_average_calc | RESULT average thermal conductivity (W/(m*K), TCON): mean result of successive thermal conductivity observations using the TCON method NOT CURRENTLY REPORTED IN EXPANDED REPORT BUT SHOULD BE | |
| TCON | RESULT | therm_con_number_calc | RESULT number of measurements (TCON): the number of measurements performed to produce the mean result for the TCON method NOT CURRENTLY REPORTED IN EXPANDED REPORT BUT SHOULD BE | |
| TCON | RESULT | therm_con_result_calc | RESULT individual thermal conductivity (W/(m*K), TCON): individual thermal conductivity measurement using the TCON method NOT CURRENTLY REPORTED IN EXPANDED REPORT BUT IT IS IN THE STANDARD REPORT | |
| TCON | RESULT | therm_con_stdev_calc | RESULT standard deviation (W/(m*K), TCON): standard deviation of the averaged results from the TCON method NOT CURRENTLY REPORTED IN EXPANDED REPORT BUT SHOULD BE | |
| TCON | SAMPLE | sample description | Sample comments | SAMPLE comment: contents of the SAMPLE.description field, usually shown on reports as "Sample comments" |
| TCON | TEST | test test_comment | Test comments | TEST comment: contents of the TEST.comment field, usually shown on reports as "Test comments" |
| TCON | RESULT | result comments | Result comments | RESULT comment: contents of a result parameter with name = "comment," usually shown on reports as "Result comments" |
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